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Fabrication and heat treatment of ceramic-reinforced aluminium matrix composites - a review
International Journal of Mechanical and Materials Engineering volume 9, Article number: 6 (2014)
Ceramic-reinforced aluminium matrix composites have attracted considerable attention in engineering applications as a result of their relatively low costs and characteristic isotropic properties. Reinforcement materials include carbides, nitrides and oxides. In an effort to achieve optimality in structure and properties of ceramic-reinforced metal matrix composites (MMCs), various fabrication and heat treatment techniques have evolved over the last 20 years. In this paper, the status of the research and development in fabrication and heat treatment techniques of ceramic-reinforced aluminium matrix composites is reviewed, with a major focus on material systems in terms of chemical compositions, weight or volume fraction, particle size of reinforcement, fabrication methods and heat treatment procedures. Various optical measurement techniques used by the researchers are highlighted. Also, limitations and needs of the technique in composite fabrication are presented in the literature. The full potential of various methods for fabricating ceramic-reinforced aluminium matrix composites is yet to be explored.
Metal matrix composites are combinations of two or more chemically non-reactive materials to form a new material system with enhanced material properties, in which titanium, aluminium and magnesium are popularly used as matrix metals and some non-metallic materials, commonly ceramics such as silicon carbide, aluminium oxide, graphite or fly ash may be used as reinforcing materials (Pandey 2004; Surappa 2003). Silicon carbide-reinforced aluminium matrix composites are advanced engineering materials with improved physical and mechanical properties as compared to their corresponding monolithic alloys. Reinforcement of particles or short fibres of SiC has proved to be advantageous since it offers the composite materials having virtually isotropic properties at low cost. In recent years, metal matrix composites find their extensive engineering application due to their high strength-to-weight ratio, stiffness and resistance to corrosion and high temperature, especially under creep conditions, for which they can be successfully used in aircraft and automobile engine technologies (Divecha et al. 1981; Weinert 1993; Khalifa and Mahmoud 2009; Reddy and Zitoun 2010b). Experimental works on SiC-based technology has gained more importance in aerospace, nuclear, automobile, chemical and cryogenic applications (Adalarasan et al. 2011). One of the major challenges during fabrication of composite material is uniform distribution of reinforcing agent in the matrix phase, which directly affects on the properties and quality of the composite material (Singla et al. 2009). Mechanical properties of a material can be tailored by subjecting it into proper heat treatment condition.
Fabrication of aluminium MMC
Hung et al. (1995) fabricated 22 wt.% SiCp-reinforced A 359 metal matrix composite (MMC) by permanent mould casting technique with an average stirring speed of 250 rpm and at pouring temperatures of 700°C to 710°C. They also fabricated 20 wt.% SiCp-reinforced L2 matrix composites by powder forming applying cold isostatic pressure of 3,700 bar for 5 min. Song et al. (1995) fabricated 20 volume fraction of SiCp (of size 3 and 20 μm) reinforced Al 2014 and Al 6061 matrix composites, and the uniformity of distribution of SiC particles in matrix material was confirmed by optical micrographs. Figure 1 shows the distribution of 20- and 3-μm SiC particles in the 6061 Al-based composites in the optical micrographs. Srivatsan and Prakash (1995) fabricated 0.2 and 0.5 volume fractions SiCp (of nominal size 16 μm) reinforced Al 2080 matrix composites at Aluminium Company of America (ALCOA), using proprietary dry blending techniques, in which the blend was cold isostatically compacted, degassed and vacuum hot pressed to produce a fully dense billet. They suggested that blending facilitates homogeneous distribution of the SiC in the matrix material. Hung et al. (1996) used 10 and 20 vol.% SiC-reinforced A 359 MMCs supplied by Duralcan (San Diego, CA, USA), fabricated by permanent mould casting at pouring temperatures of 700°C to 710°C and at an average stirring rate of 250 rpm. Sahin and Murphy (1996) used metal infiltration technique to produce SiC-coated unidirectional boron fibre-reinforced Al 2014 matrix composites, where the fibre reinforcement was in the form of wide taps made of continuous fibres placed together with titanium tape. Layers of tape were cut and stacked together in the mould to give 16 and 32 volume fractions of reinforcement. The fibre tapes were parallel to each other and continuous across the entire length of the composite plates. Xu et al. (1997) prepared two commercial composites of Al 359/SiC (10 and 20 volume fractions) by conventional stir casting treated by hot isostatic pressing (HIP) under different pressures and temperatures. Ko and Yoo (1998) fabricated hybrid metal matrix composites with SiCwhisker/SiCparticulate ratios of 1:1, 1:2 and 1:3 and single-reinforcement composites reinforced with SiCwhisker or SiCparticulate, by powder metallurgy process to compare hot deformation behaviour of the hybrid composites with that of the single-reinforcement composites. Fang et al. (1997) fabricated 16 vol.% alumina fibre-reinforced K10Mg85 Al alloy (Al + 10% Mg) matrix composite by gas pressurized liquid metal infiltration technique, which involves preheating of 16% Saffil alumina chopped fibre to 450°C and superheating of the matrix alloy melt to 850°C. A gas pressure of 3 MPa was introduced into the die cavity after pouring the melt to conduct unidirectional infiltration. They also fabricated in situ titanium diboride-reinforced Al-based composite, melting Al-4 wt.% Cu alloy to 850°C and then adding two types of compounds, K2TiF6 and KBF4, in an atomic ratio of Ti:2B by stirring. Lu et al. (1999) employed powder metallurgy process to produce Al-5% Cu/SiC MMC containing Al-Cu powder of 280 grits and SiC particles with an average particle size of 3.5 μm at a volume fraction of 15%, which were compacted by hot compression under vacuum. The defect-free and uniform distribution of SiC particles in the composite was confirmed by optical micrograph studies, which is shown in Figure 2. Manoharan and Gupta (1999) fabricated SiCp (of average size 35 μm) reinforced AA 1050 composite by disintegrated melt deposition (DMD) technique, where the properly cleaned Al alloy was heated to a temperature of 950°C and SiCp, preheated up to 950°C for 90 min, was added to it. The slurry was then mixed thoroughly for 10 min by an impeller arrangement to achieve uniform distribution of SiCp in the Al matrix. After thorough mixing, the hot composite slurry was poured into the metallic mould, during which the melt was disintegrated by two jets of argon gas oriented normal to the melt stream. Jayaram and Biswas (1999) casted Al alloy containing Si, Zn and Mg as alloying elements and fabricated SiC-reinforced Al matrix composites by melt oxidation route. The alloy was casted into flat plates and homogenized at 450°C to 500°C and the SiC preforms (mean size ranging from 5 to 300 μm), prepared by cold pressing, followed by a heat treatment at 1,200°C to 1,400°C. The alloy plate and preform are placed in contact and heated in a crucible to temperatures of 1,000°C to 1,200°C and allowed to remain at that temperature for periods of 3 to 5 days. Following cooling, the preform was removed, sectioned into specimens for mechanical tests and optical metallography. Dual process of mechanical alloying and powder metallurgy was adopted by Kwok and Lim (1999) to manufacture Al-4.5% Cu/13 vol.% SiCp composites, where high-purity aluminium (150 μm), copper (150 μm) and silicon carbide (50 μm) were mechanically alloyed in a ball mill under steady-state condition for 10 h at two different speeds of 86 and 163 rpm and the generated powders were subjected to compaction at a pressure of 420 MPa, sintered at 590°C for 5 h.
It can be clearly observed that there is slight agglomeration of SiC particulates at some places in Figure 1a, and distribution of SiC particulates is more uniform in Figure 1b. The comparison reveals that the size of reinforcement particulates is one of the influencing factors for their uniform distribution in MMC, and the distribution becomes more uniform as the particle size reduces. It can be observed that there is non-uniformity of size of SiC particulates in Figure 2. The uniformity of distribution of SiC particulates is better as compared to that of Figure 1a and slightly poor as compared to that of Figure 1b. This difference might be either due to variation of particulate size or due to variation of volume fraction of reinforcement or even might be due to variation of composition of matrix material, which is difficult to predict, since all the three parameters of the composite represented in Figure 2, i.e. matrix material (Al-5% Cu), size (average 3.5 μm) and volume fraction (15%) of reinforcement, are different as compared to those of Figure 1.
Chen et al. (2000) fabricated SiCp reinforced with A 356 alloy matrix by molten liquid aluminium stirring method, whereas Davidson and Regener (2000) manufactured 10 wt.% of SiCp-reinforced AA 6061 matrix composite by double-sided cold compaction process applying a pressure of 385 MPa for 5 min followed by pressureless sintering at 610°C for 5 h. Kumar and Dwarakadasa (2000) prepared 9% and 18% SiCp (of average particle size 40 μm) reinforced Al-Zn-Mg alloy (equivalent to Al 7075) matrix composites by liquid metal processing or stir casting technique. Figure 3 shows the size, shape and morphology of SiCp used.
Hamed et al. (2001) fabricated 10 wt.% SiCp-reinforced Al 359 composite by ingot metallurgy technique, where the Al alloy was melted at a temperature of 735°C ± 5°C and then preheated SiC particulates were added into the melt at a feed rate of 0.5 g/min and the mixture was stirred ultrasonically. The composite slurry was then poured into a preheated permanent steel mould. Cocen and Onel (2002) used melt stirring technique to prepare Al-5% Si-0.2% Mg alloy and SiC-reinforced Al-5% Si-0.2% Mg composite in an induction furnace under an argon gas protective atmosphere, whereas Borrego et al. (2002) fabricated SiC-reinforced Al 6061 matrix composite by powder metallurgy route which involves dry blending of aluminium powder with 15 vol.% of the SiC whiskers, followed by homogenization of the blends at 150 rpm for 1 h and compaction at 100°C with increasing pressure up to 300 MPa in a die. Naher et al. (2004) designed and built a new quick quench stir caster, fitted with thermocouple and temperature controller arrangement to fabricate MMC ingot. Data logger facilities were incorporated to record the temperature at a rate of 1 Hz. While fabricating SiCp-reinforced Al 356 composites using the quick quench compocasting method, he reported that full incorporation of SiC particles into the aluminium matrix can be obtained by stirring the MMC slurry in the semi-solid state without any addition of wetting agent. Zhiqiang et al. (2005) prepared SiC-reinforced Al-Si-Cu-Mg matrix composite by powder metallurgy technology, which involves compaction of powder in a cold compaction mould in a material testing machine, followed by sintering the billet in the tube furnace with electric resistance heating. Natarajan et al. (2006) fabricated SiC-reinforced A 356 composite by liquid metallurgy route, in which the alloy was melted in an electric furnace and stirred by a motorized stirrer, as a result of which a vortex was created on the top surface. Preheated SiC was added to the melt with continuous stirring, and finally, the composite slurry was poured into the cast iron mould. Fu-min et al. (2007) manufactured SiC-reinforced Al-Mg-Si matrix composite by pressureless infiltration technique in the presence of nitrogen at 850°C. Ronald et al. (2007) manufactured SiCp (50-μm size/30 volume fraction) reinforced Al 2124 alloy matrix composite through the powder metallurgy route. Figure 4 shows uniform distribution of SiC particulate in the Al 2024 matrix in SEM image.
Kalkanli and Yilmaz (2008) fabricated SiC-reinforced Al 7075 composite by the process of vertical pressure casting. In the process, first, the alloy was prepared by adding its various elements except magnesium into the induction furnace at temperatures of 750°C to 780°C. After attaining a homogeneous phase, magnesium was added followed by addition of SiC powder with continuous stirring until a highly viscous phase was obtained. The viscous fluid was then moved to a die by squeeze casting technique by applying a pressure of 80 MPa. Balogun et al. (2008) produced 5, 10, 20 and 30 vol.% of SiC (of grain sizes 240, 420, 840 and 4,200 μm) reinforced AA 6063 MMC by liquid metallurgy route in an oil fired cupola furnace with two varying charging modes using the compocasting method. Properly cleaned aluminium alloy ingots were superheated to 700°C, and SiC particulates were added to the molten metal and continuously stirred before sand casting. Kok (2008) fabricated 30 wt.% Al2O3 particle-reinforced Al 2024 alloy composites by vortex method with subsequently applied pressure of 6 MPa, using a resistance-heated furnace under argon gas. The chemical composition of the 2024 Al alloy matrix is shown in Table 1.
Mindivan et al. (2008) manufactured disc-shaped composites with 2618, 6082, 7012 and 7075 aluminium alloys as matrix and SiC as reinforcement. The process involved heating the aluminium alloy up to 800°C and SiC particles up to 1,000°C before mixing to the molten alloy. The molten SiC and alloy slurry was poured into the mould, which was preheated up to a temperature of 300°C. The mixture was hydraulically pressurized up to 600 MPa. The uniformity of distribution of SiC in the alloy was confirmed by macroscopic and microscopic examination of the composites.
Rao et al. (2009) synthesized Al-Zn-Mg-SiCp composite by solidification processing (stir casting) route which involved melting the alloy, addition of preheated SiC particles and thorough mixing. Then, the slurry was poured into the mould and allowed to cool. Hassan et al. (2009) fabricated SiC-reinforced Al-Mg-Cu composite by stir casting process, in which the aluminium ingots and copper powder were melted together at 850°C and pre-oxidized SiC powder was added to the melt. Then, Mg was added to the melt to enhance the wettability between the metal matrix and reinforcement particles. The mixture was poured into a semi-permanent steel mould and was left for air cooling. Singla et al. (2009) developed a conventional low-cost method for producing MMCs and to obtain homogenous dispersion of ceramic material. Aluminium (98.41% C.P.)/SiC (320-grit) MMC was fabricated with varying weight fractions of SiC (5%, 10%, 15%, 20%, 25% and 30%) using a two-step mixing method of stir casting technique. Scraps of aluminium were preheated at 450°C for 3 to 4 h, and SiC particles were preheated at 1,100°C for 1 to 3 h to make their surfaces oxidized. Figure 5 shows the schematic view of the furnace. The furnace temperature was then raised above the liquidus to melt the alloy scraps completely and was then cooled down just below the liquidus to keep the slurry in a semi-solid state. At this stage, the preheated SiC particles were added and mixed manually. After sufficient manual mixing, the composite slurry was reheated to fully liquid state (up to 760°C ± 10°C), and then automatic mechanical mixing was carried out for about 10 min at a normal stirring rate of 600 rpm. The position of stirrer was such that 35% of material was below the stirrer and 65% of material was above the stirrer. Crucible used for pouring of composite slurry in the sand mould was also heated up to 760°C.
Adeosun et al. (2009) fabricated 0 to 50 vol.% SiCp (1 and 60 μm) reinforced Al 1200 alloy composite in a crucible furnace; some of which were homogenized at 430°C for 8 h and air-cooled.
Khalifa and Mahmoud (2009) prepared 5, 10, and 15 wt.% of SiCp (of average size of 60 μm) reinforced Al 6063 by vortex method, which involves melting the matrix at 710°C and degassing it with dry nitrogen gas to minimize the oxidation of the molten metal. The melt was then stirred with a steel stirrer at a speed of 750 rpm for 10 to 15 min, and SiC particles, preheated to a temperature of 300°C for 2 h, were added to the vortex of molten metal during stirring. The composite slurry was poured into a metallic mould, after the stirring was completed. Bains and Manna (2010) prepared 5 and 10 vol.% SiCp (of size 100 μm) reinforced Al 6063 alloy, where the matrix alloy was preheated at 300°C for 1 to 2 h before melting and the SiCp was preheated at 300°C for 1 h before mixing to make the surface of SiCp oxidized. The furnace temperature was raised above the liquidus temperature to melt the alloy completely at 750°C and was then cooled down just below the liquidus temperature to keep the slurry in a semi-solid state. Then, the preheated SiCp were added to a semi-solid metal and mixed manually for 1 to 1.5 min. The composite slurry was then reheated to a fully liquid state, automatic mechanical mixing was done for 30 min at a stirring rate of 220 rpm and casting was done in a steel mould. Yingfei et al. (2010) produced 15 vol.% SiCp (of mean size 2 μm)/2009 Al composites through powder metallurgy technology.
Suresha and Sridhara (2010) fabricated LM 25-graphite MMC and LM 25-SiC-graphite hybrid MMC with combined weight fraction reinforcement of 2.5%, 5%, 7.5% and 10% using stir casting technique, whereas Rao et al. (2010) synthesized SiC (20 to 40 μm) reinforced AA 7009 (Al-Zn-Mg) matrix composite through solidification processing (stir casting) route which involved melting the alloy, adding preheated SiC particles in the melt by mechanical stirring and finally casting the composite melt in the preheated permanent cast iron mould. Joardar et al. (2011) prepared SiCp (of average particle size 37 μm)/LM 6 matrix composites by the stir casting route, where the aluminium alloy was melted in an electric resistance furnace having a clay graphite crucible at a temperature of 750°C. The melt was then mechanically stirred with a speed of 500 rpm by an impeller, after addition of preheated (900°C) silicon carbide particles. The pouring temperature of molten composite slurry into a sand mould was 745°C. The composition of LM 6 is tabulated in Table 2.
Alaneme (2011) developed 6, 12 and 15 vol.% of SiCp (size 30 μm) reinforced Al 6063 alloy matrix composites using a two-step stir casting method which involved melting the Al ingots and then cooling to a semi-solid state before introducing the SiC particulates and dehydrated borax mixture (in the ratio 2:1) and then stirred manually for 10 to 15 min. This was followed by heating of the mixture to 30°C above the liquidus and then performing a second stirring using a mechanical stirrer at a revolution of 300 rpm for 10 min before casting. Table 3 shows the chemical composition result of Al 6063.
Schubert and Nestler (2011) fabricated 25 vol.% SiC (of particle size ranging 2 to 3 μm) reinforced AA 2124 MMC by powder metallurgy route, where the powder is compacted by hot isostatic pressing, after a high-energy mixing process.
Kumar et al. (2012) produced SiC (of size 30 to 50 μm and weight percentage of 5, 10 and 15) reinforced Al 6061 matrix composite by liquid metallurgy technique, where the SiC was first cleaned in distilled water and dried at 90°C. It was then preheated to a temperature of 500°C and added into the vortex of molten aluminium, which was created by rotating an alumina-coated stainless steel stirrer at a speed of 550 rpm. The composite slurry was then degassed using pure nitrogen for about 3 to 4 min, and then the resulting mixture was tilt-poured into a preheated permanent mould. Alaneme and Aluko (2012) manufactured SiC (3, 6, 9 and 12 vol.%)/Al 6063 alloy matrix composites by double stir casting process, where the Al alloy billets were heated up to a temperature of 750°C and then allowed to cool to 600°C, which is slightly below the liquidus temperature, to a semi-solid state. Then, the SiC and dehydrated borax mixture (in a ratio 2:1) was added into the melt, and manual stirring of the slurry was performed for 20 min. After manual stirring, the composite slurry was reheated and maintained at a temperature of 750°C ± 10°C, and then mechanical stirring was performed for 20 min at an average stirring rate of 300 rpm. Casting was then performed in sand moulds at a pouring temperature of 720°C. Vanarotti et al. (2012) manufactured A 356/SiC composite by stir casting technique in a resistance furnace, where the matrix alloy was preheated at 450°C for 3 to 4 h and SiC particles were preheated at 1,100°C for 1 to 3 h to make their surfaces oxidized. Furnace temperature was first raised above the liquidus to melt the alloy completely and was then cooled down just below the liquidus temperature to keep the slurry in a semi-solid state. Then, the preheated SiC particles were added and mixed manually. Then, the composite slurry was reheated to a fully liquid state, i.e. up to a temperature of 730°C ± 10°C, and then automatic mechanical mixing was carried out for about 20 min at an average stirring rate of 300 rpm. The pouring temperature of the slurry to a preheated (350°C) permanent graphite mould was maintained at around 720°C. Ravesh and Garg (2012) synthesized SiC- and fly ash-reinforced Al6061 alloy composite by stir casting technique, in which the alloy was melted at 820°C in a resistance furnace. The fly ash was preheated at 400°C, and SiC was preheated at 800°C for 1 h to remove moisture and gases from the surface of the particulates. The speed of the stirrer was gradually raised to 800 rpm and the preheated reinforced particles were added with a spoon at a rate of 10 to 20 g/min into the melt with constant stirring. Then, the melt was kept in the crucible for approximate half minute in static condition, and then it was poured in the mould. Kumar et al. (2012) fabricated glass and silicon carbide particle-reinforced aluminium hybrid composite by powder metallurgy method, in which cold pressing was used for compaction of the reinforced glass-SiC aluminium hybrid composites.
Behera et al. (2012) fabricated 5, 7.5, 10 and 12.5 wt.% of SiCp (of average 400-mesh size) reinforced LM 6 alloy MMC by the liquid metal stir casting technique, where the aluminium alloy was melted to a temperature of 750°C in graphite crucible, three-phase electric resistance furnace with stirring system (shown in Figure 6). Then, 3 wt.% Mg has been added with the liquid metal. The melt was then mechanically stirred for 10 to 15 min by using an impeller at a speed of 400 to 500 rpm. During stirring, the preheated (at about 850°C to 900°C) SiC particles were introduced into the melt through the vortex of the molten metal. The composite melt was poured at a temperature of 720°C into the stepped green silica sand mould. After pouring, the melt was allowed to cool and solidify in the mould. Figure 7 shows the benchmark model of the casting. The cylindrical furnace used in their work was of electrical resistance type, having control accuracy of molten aluminium temperature of ±5°C, maximum working temperature of 1,100°C, PLC automatic temperature control, maximum stirring speed of 800 rpm and hand wheel-based manually tilting molten aluminium drain-off arrangement.
Babu and Krishnan (2012) fabricated 10 wt.% SiC and 5 wt.% B4C (both of particle size ranging from 30 to 50 μm) reinforced Al 356 metal matrix composite using stir casting method. The cleaned matrix alloy was melted in an electric arc furnace up to temperatures of 710°C to 725°C. During melting, all cover flux was added in the furnace and after complete melting of the base alloy; degassing process was carried out by adding hexachloroethane tablets. Mechanical stirring was then conducted for about 5 to 6 min at 450 rpm. SiC and B4C particles, preheated to a temperature of 790°C along with magnesium were continuously added to the melt during stirring. The molten mixture was then poured into the steel moulds. Figure 8 shows the microstructure of the SiC/B4C/Al 356 hybrid composite specimen. Table 4 shows the chemical composition test result of the hybrid composite specimen.
Kumar and Dhiman (2013) employed stir casting technique to synthesize 7 wt.% SiC (of size 27 to 33 μm) and 3 wt.% graphite (of size 20 to 25 μm) reinforced Al 7075 alloy hybrid metal matrix composites. Table 5 shows the chemical composition of the Al 7075 alloy. The matrix metal was melted above the superheating temperature, i.e. 700°C in a graphite crucible under a cover of nitrogen gas by using an electrical resistance heating furnace, and the molten metal was well agitated by a mechanical stirrer to create turbulence motion. The depth of the immersed impeller was approximately two third of the height of the molten metal from the bottom of the crucible and the speed of the stirrer maintained at 600 rpm. During mechanical stirring, 1 wt.% magnesium was added to increase the wettability of reinforcing particles. Finally, the molten metal was poured into the mild steel die, preheated to a temperature of about 300°C.
Alaneme et al. (2013) employed a two-step stir casting process for manufacturing bamboo leaf ash (BLA) and SiC-reinforced Al‐Mg‐Si alloy hybrid matrix composites with 10 wt.% reinforcements consisting of 0:10, 2:8, 3:7 and 4:6 BLA and SiC weight percentages, respectively. The bamboo leaf ash and silicon carbide particles were initially preheated separately at a temperature of 250°C. The Al alloy billets were heated to a temperature of 750°C ± 30°C to complete the molten state, followed by cooling to a semi-solid state at a temperature of about 600°C. The preheated bamboo leaf ash and SiC particles along with 0.1 wt.% magnesium were then charged into the melt at this temperature, and stirring of the slurry was performed manually for 5 to 10 min. The composite slurry was then superheated to 800°C ± 50°C and a second stirring performed using a mechanical stirrer with a stirring speed of 400 rpm for 10 min before casting into prepared sand moulds inserted with chills. Figure 9 shows the photomicrograph of Al‐Mg‐Si/2 wt.% BLA‐8 wt.% SiC hybrid composite, and Figure 10 shows the EDAX profile obtained from the Al‐Mg‐Si/2 wt.% BLA‐8 wt.% SiC hybrid composite confirming the presence of SiC, Al2O3, SiO2, Fe2O3, K2O and CaO.
Umanath et al. (2013) manufactured SiC and Al2O3-reinforced Al 6061 hybrid metal matrix composite by stir casting method, in which the Al 6061 alloy was melted in a ceramic crucible in an induction electric resistance furnace up to a temperature of 725°C and then it was degassed with nitrogen. The melt was then stirred with alumina-coated stainless steel stirrer at 600 rpm for 20 min. The immersion depth of the stirrer was maintained at about two third on the depth of the melt. During stirring, SiC and Al2O3, preheated to 600°C for 1 h, in equivalent volume fraction was added into the vortex formed due to stirring. After complete addition of the particles to the molten metal, the liquid composite was tilt-poured into the permanent steel mould, preheated at 250°C and then allowed to cool in the atmosphere. The layout of stir casting setup for composite fabrication is shown in Figure 11. Figure 12 shows the optical micrographs of (a) Al6061 alloy + 5% vol. (SiCp + Al2O3p) and (b) Al6061 alloy + 15% vol. (SiCp + Al2O3p).
Boopathi et al. (2013) prepared aluminium-SiC, aluminium-fly ash, aluminium-SiC-fly ash and aluminium-fly ash-SiC metal matrix hybrid composite by stir casting technique. The fly ash, SiC and their mixture were preheated to 300°C for 3 h to remove moisture. Pure aluminium was melted in a resistance furnace, where the melt temperature was raised up to 720°C and then the melt was stirred with the help of a mild steel turbine stirrer for 5 to 7 min at an impeller speed of 200 rpm. To increase the wettability, 1.5% of pure Mg was added with all composites. The melt temperature was maintained at 700°C during addition of Mg, SiC, fly ash and SiC-fly ash mixture particles. The dispersion of fly ash and other particles were achieved by the vortex method. The melt with reinforced particulates were poured into the preheated permanent metallic mould, and the pouring temperature was maintained at 680°C. The melt was then allowed to solidify in the mould. Figure 13 shows the stir casting unit for composite fabrication, and Figure 14 shows composite samples in the mould. Figure 15 shows the XRD spectra of the hybrid metal matrix [Al/(10% SiC + 10% fly ash)] composites.
Heat treatment of aluminium MMC
Song et al. (1995) heat-treated 20 vol.% of SiCp (of size 3 and 20 μm) reinforced Al 2014 and Al 6061 matrix composites to the T6 condition, which involved solution treatment at 530°C for 1 h, quenching in cold water and then pre-ageing at room temperature for 20 h. The materials were then aged at 50, 100, 150, 200 and 250°C for 1 h to study the effect of ageing temperature on the wear properties. Srivatsan and Prakash (1995) heat-treated the extruded SiC/Al 2080 composite billets to peak-aged T6 matrix condition, which includes solution heat treatment at 499°C for 4 h followed by cold water quenching. Subsequently, the composites were artificially aged at 177°C for 24 h. Xu et al. (1997) heat-treated hot isostatic pressed SiC/Al 359 composites to the T6 condition, which involved solution treatment for 16 h at 538°C, water quenching at above 65°C and artificial ageing for 5 h at 160°C. The optical micrographs were obtained for composite F3S.20S (20 volume fraction and of median size 12.8 ± 1.0 μm of SiCp-reinforced AA 359 matrix composite) in as-cast condition and in HIP condition as shown in Figure 16a,b. Large pores are observed in the microstructure of as-cast composite; however, the porosity levels reduced effectively up to below 0.5% after the HIP treatment of the composite. The reduction of porosity level was claimed for the diffusion bonding of adjacent pore surfaces as the composites were under high isostatic pressure and temperature during the HIP treatment.
Kwok and Lim (1999) solution-treated Al/SiC composites at 515°C for 4 h in a muffle furnace and then quenched them to room temperature, and finally, ageing was carried out at a temperature of 175°C for 17 h. Chen et al. (2000) heat-treated Al 356/SiCp composites to T6 condition at a temperature of 535°C ± 5°C for 6 h and then quenched them in water at 80°C. Finally, they were aged at a temperature of 200°C for 5 h in air. Davidson and Regener (2000) solution-treated SiCp/AA 6061 composites at 530°C for 1 h and then quenched them in cold water, followed by ageing for 8 h at 175°C. Hamed et al. (2001) subjected SiCp-reinforced Al 359 composite to T6 heat treatment which involved solution treatment for 16 h at 530°C, quenching at 60°C and then ageing for 9 h at 160°C. Figure 17 shows the microstructures of the heat-treated 359/SiC/10p composite materials.
A more uniform distribution of SiC particulates are observed in the microstructural image shown in Figure 17 as compared to that in Figure 16a, which clearly depicts the positive effect of heat treatment on uniformity in the distribution of reinforced ceramic particles in metal matrix composites.
Davim (2003) heat-treated, solutionized and aged A 356/20 vol.% SiCp (of average dimension about 20 μm) composites at T6 condition for 5 h at 154°C to conduct turning experiments. Kalkanli and Yilmaz (2008) heat-treated SiC/Al 7075 composites according to ASM T6 heat treatment conditions, followed by solutionization at 480°C for 55 to 65 min. Then, they were quenched and precipitation heat treated at 120°C for 24 h. Balogun et al. (2008) heat-treated Al 6063/SiC metal matrix composite at 415°C for 1-h soak time. Khalifa and Mahmoud (2009) solution heat-treated the as-cast and extruded SiC/Al 6063 composite samples at 530 ± 3°C for 3 h and then quenched them in cold water. After cooling, specimens were artificially aged at 175 ± 1°C to determine the peak hardness level attainable during age hardening and the time required for achieving such a hardness level. Rao et al. (2010) heat-treated SiC/Al 7009 composites in three stages, i.e. solution treatment for 8 h at 490°C, then quenching in water and finally artificial ageing at a temperature of 180°C for 4, 6, 8 and 10 h in order to get the better properties. Alaneme (2011) utilized four different temperature conditions to SiCp/Al 6063 composites, i.e. as-cast condition, and three others developed by heat treatment, namely solutionized and water quenched, artificially age hardened at 180°C and artificially age hardened at 195°C. The solutionized and quenched temperature was achieved by solutionizing the samples at 550°C for 3 h and then quenching in water. The two artificial ageing temperatures were achieved by initially solutionizing at 550°C for 3 h followed by water quenching. Age hardening treatments were performed at 180°C and 195°C for 2 h before water quenching. Alaneme and Aluko (2012) conducted solution treatment of SiC/Al 6063 composite samples in the furnace at 560°C for 2 h, followed by water quenching. Ageing was then performed at 180°C for 3 h, followed by water quenching. The optical micrographs obtained for as-cast Al 6063/9 vol.% SiCp (of particle size 30 μm) composite and heat-treated (solution treatment followed by age hardening) Al 6063/9 vol% SiCp (of particle size 30 μm) composite are depicted in Figure 18a,b, respectively. Some localized clustering of SiC particles was observed in as-cast composite, whereas a more homogeneous distribution of the SiC particles was achieved in heat-treated composite. Another interesting conclusion from this comparison was that the volume percentage of silicon carbide reinforcement did not influence the pattern of distribution of SiC under as-cast and solution-treated followed by age-hardened conditions of composites.
Kumar and Dhiman (2013) performed T6 heat treatment of SiC/Gr/Al 7075 hybrid metal matrix composite specimens, in which the solution treatment was done at 490°C for 2 h, followed by water quenching, and ageing treatment was done at 120°C for 20 h.
After extensive literature study, it was observed that researchers adopt either powder metallurgy or molten metal stir casting technique, mostly the later one, for fabrication of ceramic-reinforced aluminium matrix composites, which may be due to the economical viability of this method. The technique has been summarized through eight steps.
Step 1. Selection of matrix metal and reinforcing agent
Any type of aluminium alloy may be chosen as matrix metal depending upon the application of the composite. Silicon carbide particulates have widely been used as reinforcing element; however, the use of aluminium oxide, boron carbide, graphite, fly ash and bamboo leaf ash also find their application as reinforcing agent during fabrication of aluminium matrix composites.
The size of SiC particulate chosen for reinforcement differs within a wide range, even from very fine size of 1 μm to coarse size of 4,200 μm. For instance, very fine SiC particulate sizes of 1, 2, 3, 3.5 and 5 μm were used by Adeosun et al. (2009), Yingfei et al. (2010), Schubert and Nestler (2011), Song et al. (1995), Lu et al. (1999) and Jayaram and Biswas (1999), respectively, whereas researchers like Kalkanli and Yilmaz (2008) and Jayaram and Biswas (1999) tried with coarse SiC particulate sizes of 240, 300, 420, 840 and 4,200 μm for manufacturing Al matrix composites. However, particulate size of SiC used by majority of the researchers ranges in between 30 and 60 μm.
Step 2. Determination of weight/volume fraction of reinforcement
The amount of SiC particles added to the matrix alloy is calculated either in the form of weight fraction or volume fraction of the composite. Low weight fractions of SiC (like 2.5%, 5% and 7.5%) have been used by Suresha and Sridhara (2010), Singla et al. (2009) and Kumar et al. (2012), whereas high weight fractions (like 20%, 22%, 25% and 30%) have also been used for fabrication of AMCs by Hung et al. (1995) and Singla et al. (2009). Majority of the researchers use moderate value weight fractions (10% to 15%) of SiC to fabricate AMCs. Similarly, volume fractions of SiC used vary from very low values like 0.2%, 0.5%, 3%, 5% and 6% (Srivatsan and Prakash 1995; Alaneme and Aluko 2012; Kalkanli and Yilmaz 2008; Alaneme 2011) up to high values like 20%, 25% and 30% (Kalkanli and Yilmaz 2008; Schubert and Nestler 2011) through intermediate values like 10%, 12% and 15%.
Step 3. Preheating and/or melting of matrix alloy
During fabrication of Al matrix composite, some researchers preheated the properly cleaned matrix alloy by distilled water (Kumar et al. 2012) or acetone (Babu and Krishnan 2012) up to a temperature of 450°C for 3 to 4 h (Singla et al. 2009), 300°C for 1 to 2 h (Khalifa and Mahmoud 2009), 500°C (Kumar et al. 2012) or 450°C for 3 to 4 h (Vanarotti et al. 2012) to make its surface oxidized. The preheating of matrix alloy was not conducted by a number of researchers; however, they have directly gone for melting the alloy above its liquidus temperature. During melting of matrix alloy, the temperature may be maintained in the range of 700°C to 950°C. Most of the investigators have melted the Al alloy in the temperature range of 700°C to 800°C (Hamed et al. 2001; Kalkanli and Yilmaz 2008; Singla et al. 2009; Khalifa and Mahmoud 2009; Kumar and Dhiman 2013; Alaneme et al. 2013 and many more); however, some investigators have also gone beyond 800°C (Manoharan and Gupta 1999; Hassan et al. 2009; Ravesh and Garg 2012). Cocen and Onel (2002) and Kok (2008) melted Al alloy under argon gas protective atmosphere; however, Kumar and Dhiman (2013) used nitrogen gas during melting of Al alloy.
Step 4. Addition of all cover flux during melting and degasser after melting
During melting, the charge is to be fluxed with all cover flux or coverall to prevent dressing. The molten alloy is to be degasified by some suitable degasser, like tetrachlorethane or hexachloroethane or pure nitrogen gas, to minimize oxidation of molten metal (Khalifa and Mahmoud 2009; Babu and Krishnan 2012; Kumar et al. 2012; Reddy and Zitoun 2010a).
Step 5. Preheating of reinforcement
The SiC particulates are to be preheated up to a certain temperature for 1 to 3 h before adding them into the molten Al alloy. Singla et al. (2009), Bains and Manna (2010) and Vanarotti et al. (2012) claim that preheating of reinforcing particles is necessary to get their surface oxidized; however, Manoharan and Gupta (1999), Ravesh and Garg (2012) Alaneme et al. (2013) and Boopathi et al. (2013) claim that preheating is necessary to remove moisture from reinforcing particulates and to improve wettability in matrix material. The temperature of preheating was ranged in between 300°C and 1,100°C (Khalifa and Mahmoud 2009; Bains and Manna 2010; Joardar et al. 2011; Behera et al. 2012 and many more).
Step 6. Manual/motorized stirring, addition of preheated reinforcing agent and wetting agent and temperature control of the abrasive slurry
As per some researchers (Natarajan et al. 2006; Kumar et al. 2012; Behera et al. 2012; Umanath et al. 2013), motorized stirring may be performed to molten aluminium and preheated SiC along with some suitable wetting agent may be added to the vortex created on the surface of molten aluminium due to continuous stirring, whereas some other researchers (Singla et al. 2009; Khalifa and Mahmoud 2009; Alaneme 2011; Alaneme and Aluko 2012; Vanarotti et al. 2012; Alaneme et al. 2013) are in favour of addition of preheated SiC along with wetting agent to the aluminium at semi-solid state, which can be achieved by cooling down the temperature of molten metal just below its melting point. After addition of preheated SiC particles and wetting agent to semi-solid aluminium, sufficient manual stirring is to be performed for 10 to 20 min to avoid difficulty of motorized mixing in the semi-solid state of the alloy. Thorough mixing of the slurry is required to achieve uniform distribution of SiCp in the Al matrix. Naher et al. (2004) reported that stirring the MMC slurry in semi-solid state, during the solidification process, helps to incorporate ceramic particles into the alloy matrix without any addition of wetting agent. After sufficient manual mixing, the composite slurry is reheated to fully liquid state and then automatic mechanical mixing is to be carried out for 10 to 20 min. The mechanical stirring speed used are 220 rpm (Bains and Manna 2010), 300 rpm (Alaneme 2011, Alaneme and Aluko 2012; Vanarotti et al. 2012), 400 rpm (Alaneme et al. 2013), 600 rpm (Singla et al. 2009) and even ultrasonic (Hamed et al. 2001). Preheated SiC may be added at very slow rate, for example, 0.5 g/min (Hamed et al. 2001), 5 g/min (Kalkanli and Yilmaz 2008) or 10 to 20 g/min (Ravesh and Garg 2012). To prevent iron contamination in the abrasive slurry, the stirrer system may be coated with Zirtex 25 (Manoharan and Gupta 1999) or alumina (Kumar et al. 2012; Umanath et al. 2013).
After addition of preheated SiC to the molten Al alloy or to semi-solid Al alloy, as the case may be, some suitable wetting agent of required weight percentage is to be added and to be mixed thoroughly. Addition of wetting agent is required to achieve a strong bonding between the matrix alloy and the reinforcement particles by decreasing the surface energy (wetting angle) between them. Pure magnesium powder or borax may be used as wetting agent for the purpose. Addition of pure magnesium also enhances the fluidity of the molten metal. Behera et al. (2012) added 3 wt.% of magnesium and Ozben et al. (2008) added 2 wt.% of magnesium; however, Kumar and Dhiman (2013) added 1 wt.% of magnesium as wetting agent and stated that addition of magnesium has two benefits, i.e. it acts as an alloying element and it reduces the surface tension thus improving wetting dispersion. Babu and Krishnan (2012) added magnesium in order to compensate for its losses during melting and for wetting purposes. Alaneme and Aluko (2012) used borax as wetting agent and added SiC and borax (dehydrated by heating at 250°C for 20 min) mixture in the ratio 2:1, during fabrication of AMCs.
Step 8. Pouring the abrasive slurry to preheated mould
After sufficient mechanical mixing for about 10 to 20 min, the abrasive slurry is transferred to preheated mould, which may be made of sand, ceramic, cast iron or steel. The mould may be preheated up to a temperature within the range of 250°C to 760°C (Umanath et al. 2013; Kumar and Dhiman 2013; Vanarotti et al. 2012; Kalkanli and Yilmaz 2008; Singla et al. 2009), whereas the pouring temperature of molten abrasive slurry is maintained in the range of 680°C to 750°C (Boopathi et al. 2013; Hung et al. 1995; Kalkanli and Yilmaz 2008; Alaneme and Aluko 2012; Vanarotti et al. 2012; Joardar et al. 2011). After pouring molten abrasive slurry into the mould cavity, it is allowed to cool to atmospheric condition at different cooling rates.
Most of the researchers follow T6 condition of heat treatment for SiC-reinforced Al matrix composite, which involves solution treatment at a certain temperature for a certain period of time, quenching in water followed by ageing at a certain temperature for a certain duration. The solution treatment temperature and time and the ageing temperature and time depend upon the type of the Al alloy used for composite fabrication.
An attempt has been done to outline various methods of fabrications of aluminium matrix composite, giving special emphasis to stir casting method. Various steps involved in this method has been discussed briefly, and emphasis has been given to different key points, such as selection of weight or volume fraction of SiC in the composite, SiC particulate size, preheating temperature of SiC, preheating and melting temperature of Al matrix, stirring speed during agitation of the composite slurry, use of flux, degasser and wetting agent, preheating temperature of the mould and pouring temperature of composite slurry into the mould. T6 condition of heat treatment for composites of various Al alloy has been outlined briefly.
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The authors declare that they have no competing interests.
DKD performed thoroughly the literature on fabrication of MMCs and carried out fabrication of MMCs by stir casting method. PCM studied characterization of MMCs by various techniques including Mechanical tests, physical tests and optical tests. SS participated in the sequence alignment and drafted the manuscript. SP participated in the sequence alignment and drafted the manuscript. All authors read and approved the final manuscript.
Dipti Kanta Das, Saranjit Singh and Swati Pattanaik are authors contributed equally to this manuscript.
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Das, D.K., Mishra, P.C., Singh, S. et al. Fabrication and heat treatment of ceramic-reinforced aluminium matrix composites - a review. Int J Mech Mater Eng 9, 6 (2014). https://doi.org/10.1186/s40712-014-0006-7
- Permanent mould technique
- Stir casting
- ASM T6
- Aluminium matrix composites
- Heat treatment